Nozzles for Focusing Aerosol Particles

These nozzles aerodynamically focus aerosol particles into a small-diameter jet.

Several nozzles have been designed to aerodynamically focus aerosol particles into a small-diameter jet, so that individual particles can be illuminated by a laser beam and their light scattering and/or laser-induced fluorescence (LIF) spectra can be measured. An additional nozzle can aerodynamically puff selected particles out of the airstream so that they can be sorted and collected.

In single-particle LIF and elastic scattering measurements, it is desirable that the particles be focused into as narrow a stream as possible (as small as 20 μm diameter), and for the particles to remain collimated for a distance of a few millimeters. Particles having different sizes and shapes should flow at the same speed and the same trajectory in the particle stream as it moves away from the nozzle. To help the particles flow in a collimated stream, an eduction tube was used a short distance (about 1 cm) below the nozzle.

The first aerodynamic focusing nozzle was a single-piece nozzle that looks similar to a 30° cone. Originally, plastic glass was used to make the nozzle, but it did not work well, possibly because of static charges. The first nozzle that worked well was machined from aluminum. This nozzle produces a laminar aerosol flow with an aerosol jet diameter of a few hundred microns at a flow rate of 0.6 to 2.1 L/min. Individual aerosol particles (1 to 10 mm size) within the jet move at about 10 m/s when the flow is nominally 1 L/min.

The second-generation nozzle was designed to measure two-dimensional angular optical scattering (TAOS) over very large angles using an elliptical mirror. In this setup, the laser and particle interrogation region (located at the mirror focal point) is located well below (more than 1") the nozzle exit. At this distance, the aerosol stream is no longer well focused. The nozzle assembly was modified so that it could be inserted into the relatively small (0.40") opening of the mirror and close to the mirror focal point. This nozzle functions similarly to the first-generation nozzle, but with a better focusing capability.

The third-generation nozzle assembly was developed with a sheath flow. The inner nozzle of the assembly has similar design to the second-generation nozzle, but with a separate outer nozzle for a clean-air sheath flow. This nozzle can produce a tightly focused aerosol jet of particles having relatively uniform speed over distances of more than 5 mm. The nozzle provides for a well-defined interrogation region, and also prevents the contamination of optics by preventing sampled aerosol from circulating in the optical cell.

The machining process posed a particular challenge, because the inner surfaces needed to be joined smoothly, with no abrupt changes in curvature, and the exit hole needed to be small (0.9-mm diameter). The external portions of the nozzles were machined in a more conventional manner using computer numerical control (CNC) lathes and milling machines running programs written by computer-aided machining (CAM) software. The close tolerance of concentricity of the two nozzles was achieved by placing a perforated ring at the end of the inner nozzle. This ring formed a close sliding fit to the outer nozzle. Fabrication of the nozzle with the desired shape was accomplished using EDM technology. First, a copper tungsten electrode was turned on a CNC lathe. The geometry of the electrode matched that of the inner surface to be machined. Next, the electrode was precisely aligned over the nozzle, and the EDM process initiated. Roughing and finishing electrodes were used to produce the desired finish on the inside surface.

This work was done by Yong-Le Pan, John Bowersett, Steven C. Hill, Ronald G. Pinnick, and Richard K. Chang of the Army Research Laboratory. For more information, download the Technical Support Package (free white paper) at www.defensetechbriefs.com/tsp  under the Mechanics/Machinery category. ARL-0099



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Nozzles for Focusing Aerosol Particles

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Defense Tech Briefs Magazine

This article first appeared in the December, 2010 issue of Defense Tech Briefs Magazine (Vol. 4 No. 6).

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Overview

The document titled "Nozzles for Focusing Aerosol Particles" is a final report authored by Yong-Le Pan, John Bowersett, Steven C. Hill, Ronald G. Pinnick, and Rickard K. Chang, published in October 2009 by the U.S. Army Research Laboratory. The report focuses on the design, fabrication, and testing of specialized nozzles intended for single-particle sampling measurements, particularly in the context of laser-induced fluorescence and two-dimensional angular optical scattering.

The primary objective of the research is to improve the efficiency and accuracy of aerosol particle sampling, which is crucial for various applications, including environmental monitoring, health assessments, and military operations. The report details the development of both single-piece nozzles and a two-piece nozzle that incorporates a sheath flow, which enhances the aerodynamic focusing of particles. This design aims to optimize the collection and analysis of atmospheric particles, including bioaerosols.

The authors provide a comprehensive overview of the nozzle designs, including their operational principles and the methodologies employed in their testing. The report highlights the significance of aerodynamic focusing in achieving high-resolution measurements of aerosol particles, which can be challenging due to their small size and the complexities of their behavior in different environments.

In addition to the technical specifications and performance evaluations of the nozzles, the report includes an abstract summarizing the key findings and implications of the research. The findings are presented in a manner that emphasizes their relevance to both scientific inquiry and practical applications in fields such as environmental science and public health.

The document is unclassified and approved for public release, indicating its accessibility to a broader audience interested in aerosol research and related technologies. It serves as a valuable resource for researchers, engineers, and policymakers involved in the study and management of aerosol particles.

Overall, this report contributes to the understanding of aerosol dynamics and provides innovative solutions for enhancing particle sampling techniques, thereby advancing the field of aerosol science and its applications.