Case Study Supreme 10HT

Overview

This case study details the application and performance of Master Bond Supreme 10HT, a high-performance epoxy adhesive used in demanding industries such as aerospace, electronics packaging, and capacitor tank sealing. Supreme 10HT is recognized for its exceptional strength, durability, and thermal stability across wide temperature ranges and after repeated thermal cycling.

In electronics packaging, especially for high-temperature control modules like automotive Engine Control Units operating above 175°C, Supreme 10HT demonstrated reliable die-to-substrate bonding. Tests conducted at EPFL showed that Supreme 10HT bonds strengthened after heat exposure up to 1000 hours at 210°C, maintaining forces above military standard requirements despite some strength reduction after extended heating.

For capacitor tanks, which require durable seals between metallic components and insulating bushings under harsh environmental conditions, Supreme 10HT provided robust lap shear strength at both elevated (75°C–90°C) and room temperatures. Its compatibility with aromatic dielectric fluids was confirmed by exposure tests at 75°C for two weeks without adverse effects on dielectric properties, indicating its suitability to ensure long-term sealing performance in power distribution systems that operate outdoors.

A significant focus was on supersonic aircraft adhesive joints subject to extreme temperatures from -55°C to 200°C. Adhesives designed for low temperatures often soften or degrade at high temperatures, while high-temperature adhesives are brittle when cold. Research by the University of Porto and University of Bristol explored mixed-adhesive joints combining Supreme 10HT as the low-temperature adhesive with a high-temperature bismaleimide adhesive. Results showed Supreme 10HT maintained stiffness, strength, and ductility from -55°C up to 100°C and softened above its Tg (~135-140°C). Mixed joints improved overall strength across the temperature range, indicating that Supreme 10HT supports loads effectively at low to moderate temperatures, while the bismaleimide handles higher temperatures.

Additional tests revealed no bond strength degradation in Supreme 10HT samples after 10 and 100 thermal cycles between 20°C and 180°C, demonstrating high thermal fatigue resistance.

In conclusion, Supreme 10HT combines excellent mechanical performance, thermal durability, and environmental resistance, making it a versatile adhesive choice for aerospace, automotive, electronics, military/defense, and other sectors requiring reliable bonding and sealing under challenging conditions.

References include peer-reviewed studies and patents validating these findings.